Make a sketch, roughly to scale, of the 1H NMR spectrum expected for an AX spin system with δA = 1.00, δX = 2.00, and JAX = 10 Hz recorded on a spectrometer operating at (i) 250 MHz, (ii) 800 MHz. The horizontal scale should be in hertz, taking the resonance from TMS as the origin.

Make a sketch, roughly to scale, of the 1H NMR spectrum expected for an AX spin system with δA = 1.00, δX = 2.00, and JAX = 10 Hz recorded on a spectrometer operating at (i) 250 MHz, (ii) 800 MHz. The horizontal scale should be in hertz, taking the resonance from TMS as the origin.

Organic Chemistry

8th Edition

ISBN:9781305580350

Author:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote

Publisher:William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote

Chapter13: Nuclear Magnetic Resonance Spectroscopy

Section: Chapter Questions

Problem 13.28P

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Question

Make a sketch, roughly to scale, of the ¹H NMR spectrum expected for an AX spin system with δ_A = 1.00, δ_X = 2.00, and J_AX = 10 Hz recorded on a spectrometer operating at (i) 250 MHz, (ii) 800 MHz. The horizontal scale should be in hertz, taking the resonance from TMS as the origin.

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