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You modified a workup from a multi-step synthesis, making the compound below. The crude compound is then dissolved in CH₂Cl₂. After that you extract with H₂O x 2, NaOCI x 2, water and then brine, then the organic layer was dried by Na₂SO4. OH Upon evaporation of your dichloromethane solution, you find your yield of alcohol Is close to 0%. Assume that you had performed the reaction and extractions well (i.e. you didn't spill anything or pick up the wrong layer). Why was your yield of product so low?

You modified a workup from a multi-step synthesis, making the compound below. The crude compound is then dissolved in CH₂Cl₂. After that you extract with H₂O x 2, NaOCI x 2, water and then brine, then the organic layer was dried by Na₂SO4. OH Upon evaporation of your dichloromethane solution, you find your yield of alcohol Is close to 0%. Assume that you had performed the reaction and extractions well (i.e. you didn't spill anything or pick up the wrong layer). Why was your yield of product so low?

Chemistry
Chemistry
10th Edition
ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Chapter1: Chemical Foundations
Section: Chapter Questions
Problem 1RQ: Define and explain the differences between the following terms. a. law and theory b. theory and...
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You modified a workup from a multi-step synthesis, making the compound below. The crude compound is then dissolved in CH₂Cl₂. After that you extract with H₂O x 2, NaOCI x 2, water and then brine, then the organic layer was dried by Na₂SO4. OH Upon evaporation of your dichloromethane solution, you find your yield of alcohol Is close to 0%. Assume that you had performed the reaction and extractions well (i.e. you didn't spill anything or pick up the wrong layer). Why was your yield of product so low?
Transcribed Image Text:You modified a workup from a multi-step synthesis, making the compound below. The crude compound is then dissolved in CH₂Cl₂. After that you extract with H₂O x 2, NaOCI x 2, water and then brine, then the organic layer was dried by Na₂SO4. OH Upon evaporation of your dichloromethane solution, you find your yield of alcohol Is close to 0%. Assume that you had performed the reaction and extractions well (i.e. you didn't spill anything or pick up the wrong layer). Why was your yield of product so low?
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