What spectral features would you expect to see in MS and IR to determine whether the synthesis was fully successful/complete?

Chemistry & Chemical Reactivity
10th Edition
ISBN:9781337399074
Author:John C. Kotz, Paul M. Treichel, John Townsend, David Treichel
Publisher:John C. Kotz, Paul M. Treichel, John Townsend, David Treichel
Chapter5: Principles Of Chemical Reactivity: Energy And Chemical Reactions
Section5.8: Product- Or Reactant-favored Reactions And Thermodynamics
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What spectral features would you expect to see in MS and IR to determine whether the synthesis was fully successful/complete?

Н он
H
H2N-
H2N-
Ni(CIO4)2
N.
+
HN
N Ni2* HN´ 2 CIO,
N N2* HN
2 CIO,
'N N2* HN
2 CIO,
H20-ELOH
reflux
H2N.
N.
H
H
H.
Transcribed Image Text:Н он H H2N- H2N- Ni(CIO4)2 N. + HN N Ni2* HN´ 2 CIO, N N2* HN 2 CIO, 'N N2* HN 2 CIO, H20-ELOH reflux H2N. N. H H H.
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