Synthesis of Dihydrosafrole via Friedel-Crafts Acylation & Reduction Experiment resulting in following IR spectra. Can you analyze it and fill the following table? Are their any impurities found?

Chemistry
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ISBN:9781305957404
Author:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
Publisher:Steven S. Zumdahl, Susan A. Zumdahl, Donald J. DeCoste
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Attached 2nd Reaction was performed in the Synthesis of Dihydrosafrole via Friedel-Crafts Acylation & Reduction Experiment resulting in following IR spectra. Can you analyze it and fill the following table? Are their any impurities found? 

Peak Position cm-1

Bond Type

Functional Group

     
     
     
     
     
     
     
     
     
     
Reaction 2
CH₁
Catalytic Pd/Alumina
PMHDS (H-SIR, Source)
Methanol
.CH,
Transcribed Image Text:Reaction 2 CH₁ Catalytic Pd/Alumina PMHDS (H-SIR, Source) Methanol .CH,
4000
3500
3000
2500
Wavenumbers (cm-1)
2000
1500
1000
500
-5-
0-
1503.63
1487.08
1441.26
2962.30
2932.17
2874.99
1247.27
1119.13
1101.55.
1086.79
416.51
1040.35
5-
932.96
808.92
10-
15-
1186.97
565.81
20-
25-
%Transmittance
2823.03
1377.47
1465.10
1328.07
791.17
1203.34
3012.14
1608.97
865.50 887.73
633.14
45-
2776.30
3070.45
50-
665.31
769.12
55-
1630.28
1862.27
1748.81
1707.65
1684.64
3582.77
-09
1297.65
7285259
-99
2609.32
70-
2301.72
2167.76
2042.43
Transcribed Image Text:4000 3500 3000 2500 Wavenumbers (cm-1) 2000 1500 1000 500 -5- 0- 1503.63 1487.08 1441.26 2962.30 2932.17 2874.99 1247.27 1119.13 1101.55. 1086.79 416.51 1040.35 5- 932.96 808.92 10- 15- 1186.97 565.81 20- 25- %Transmittance 2823.03 1377.47 1465.10 1328.07 791.17 1203.34 3012.14 1608.97 865.50 887.73 633.14 45- 2776.30 3070.45 50- 665.31 769.12 55- 1630.28 1862.27 1748.81 1707.65 1684.64 3582.77 -09 1297.65 7285259 -99 2609.32 70- 2301.72 2167.76 2042.43
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