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- Show how you will useModified Gabriel’s Synthesis and Streckers’s Synthesis to prepare phenylalanine in the laboratory.tert-Butoxycarbonyl azide was developed as a reagent for peptide synthesis at OWL's home institution, the University of Massachusetts, by Prof. L.A. Carpino. It is prepared by treating tert-butoxycarbonyl chloride with sodium azide. Propose a structure for the initially-formed intermediate in this reaction.Suggest a test you will use to show that a given food substance contains protein. Show how you will use; A modified Gabriel's synthesis A Streckers' synthesis to prepare phenylalanine in the laboratory.
- Synthesize the compund (Amlodipine) via Hantzsch dihydropyridine synthesis.(D)The best route to synthesise aromatic primary amines is by reduction of the corresponding nitro compounds. Draw the reaction scheme for the preparation of p-toluidine.From the given structures which is(a) an acid halide? (b) a secondary amide (c) an aldehyde incapable of self-aldol consensation?
- (a) Vanillic acid is a phenolic compound found in vanilla and many other plant extracts. It is a flavouring and scent agent that produces a pleasant, creamy odour. Show the biosynthesis route for the formation vannillic acid from phenylalanine (Shikimate pathway). HO. NH2 Phenylalanine Vanillic acidFollowing is an outline of a synthesis of the bronchodilator carbuterol, a beta-2 adrenergic blocker with high selectivity for airway smooth muscle receptors. Q.Suggest a structural relationship between carbuterol and ephedrineDraw the expected product of the reaction of the following sugars with excess methyliodide and silver oxide.(a) a-d-fructofuranose (b) b-d-galactopyranose