V6 Aldol Condensation: The Synthesis of 2'-Hydroxy-4-methoxychalcone25 mg of your product and dissolve in MeOH (50 mL) using a 50 mL volumetric flask – stock solution. Take 0.5mL of the stock solution and make up (in a volumetric flask) to 25 mL – Solution A. Take 5 ml of solution A andmake up to 25 mL with MeOH – solution B- and record spectrum. Then take 1 mL of solution A and make upto 25 mL with MeOH – solution C- and again record spectrum. Plot the value of the absorbance at the Amaxversus concentration and using the Beer-Lambert relationship (Abs ɛcl)calculate the extinction coefficient (ɛ) and please show graph ABS人marA•3321-062B .3650.296C .3770.078

The amount of solute that dissolves in a calculated volume of the solvent to yield a solution is…

Answered: Aldol Condensation: The Synthesis of…

Organic Chemistry

9th Edition

ISBN:9781305080485

Author:John E. McMurry

Publisher:John E. McMurry

Chapter18: Ethers And Epoxides; Thiols And Sulfides

Section18.SE: Something Extra

Problem 62GP: The Zeisel method is an old analytical procedure for determining the number of methoxyl groups in a...

See similar textbooks

Similar questions

Please pronde ne approprate reagents or product. 1.Os0y,TBHP, H20/THF -> 2. TSOH, acetone, PhH,neat 3. AICI3, CH3COCI, CH2C12 2) 1. B200B2,NBS, CC14> 2. Mg, THF;then Pa°Ln, PhBr 3. HNO3 , HzSo4 4. 2n, HCI me Br Me0 (3 meo MeN HN Meo me Br
6. Provide reagents and intermediates in the indicated boxes to complete the reaction scheme. + H NaBH3CN, HCI (two steps, no acidic hydrolysis, from one product) 016H (w/o heat) 1. MeLi (xs) 2. HCI, H₂O NH₂ 1. Saponification 2. A 0 1. MeMgBr (xs) 2. HCI, H₂O 018 Me NH₂ 1. Dibal H, 2. H3O+ POCk3, pyr or + 1. LIAIH(O'Bu)3 (XS) 2. acidic workup
In each reaction box, place the best reagent and conditions from the list provided. 1) Br 2) 3) 4) DEET (the active ingredient in over the counter insect repellant) 5) Answer Bank Mg, Et,0 HN(CH, CH, ), (1 equiv.) H,O* CH,COOH CH,CH,NH, CH,CH, Br NH(CH,CH,),(2 cquiv.) НСООСH, H,CO НСООН CH, CH, OH NaCN NaNH, Br,, FeBr, SOCI, CO,
4. Predict the product for each reaction. Note that some have two reactions. You can give the final answer or use mechanisms to arrive at the correct answer. NH₂ Ph P KCN HBr 0₂ Me₂S OH KMnO4 I j H H+ H₂O H₂O* (COCI),, DMSO Et₂N OH Ph₂P= H₂NNH₂ HO H₂O* Дон H* 'OH alm OH H₂O* H₂O* NaBH MeOH NaBH EtOH
Chemist 4:22 PM Thu Jun 16 ... @日 HW2 Synth Aromaticity - x CHEM220 SU exam_dhill Course Notes Unit 3 B 2 N U ★ P {T} DA 6) Synthesis: Design a reasonable synthesis for the following: Br p= OH NOTE: You can use any other inorganic reagent, but no other organic reagents. The molecule below is provided as a possible intermediate to go through in the synthesis. It is not required that you make the molecule below in your synthesis. classNotes x HW2 Synth Aromati... x 35% Homework 2 E
15) Propose a synthetic route to convert 3-methyl-1-butanol into 3-methyl-2-butanol. OH OH A) 1. NaOH; 2. H3O+ B) 1. H₂SO4, heat; 2. NaBH4; 3. H3O+ C) 1. H2SO4, heat; 2. Hg(OAc)2, H2O; 3. NaBH4 D) 1. Hg(OAc)2, H2O; 2. H2SO4, heat; 3. NaBH4 E) 1. NaOMe; 2. BH3-THF; 3. H2O2, NaOH Answer: C
The Zeisel method is an old analytical procedure for determining the number of methoxyl groups in a compound. A weighed amount of the compound is heated with concentrated HI, ether cleavage occurs, and the iodomethane product is distilled off and passed into an alcohol solution of AgNO3, where it reacts to form a precipitate of silver iodide. The Agl is then collected and weighed, and the percentage of methoxyl groups in the sample is thereby determined. For example, 1.06 g of vanillin, the material responsible for the characteristic odor of vanilla, yields 1.60 g of Agl. If vanillin has a molecular weight of 152, how many methoxyl groups does it contain?
What is the product of the following reaction sequence? 1) MeMgBr (excess) 2) Hа0 HO SOCI2 H2SO4, heat ОН I. I. LOH OH II. IV. O i. only iii. only none of the other answer choices are correct O ii. only O iv. only
Help In finding the major organic products for these reactions + NaOCH2CH3 1. add slowly 2. HCI b) 1. NaOCH, CH3OH 2. (CH3)2CHCH2CH₂Br 3. H3O+, heat
Choose the best reagents to complete the reaction shown below. HO 0= 0= OH e A B C D E 1.03 2. HOẠC mCPBA 2. H3O+ 1. Hg(OAc)2, H₂O 2. NaBH4, NaOH RCO3H 1. OsO4 (catalytic),
Choose the best reagents to complete the reaction shown below. A B C E D HO о O= OH RCO₂H 1. OsO4 (catalytic) 2. NMO 1. KMnO4, OH- (warm) 2. H₂O* MCPBA 2. H3O+ 1. Hg(OAc)2, H2O E 2. NaBH4, NaOH Q Q
ucf.edu/courses/1379813/quizzes). Question 12 Identify the major product from the following series of reactions. 1. NaOEt 1. NaOEt 2. CH3CH2CI OEt 2. H30*, Quendch 3. H30*, Heat но он HO H.

SEE MORE QUESTIONS

Recommended textbooks for you

Organic Chemistry

Chemistry

ISBN:

9781305080485

Author:

John E. McMurry

Publisher:

Cengage Learning

Organic Chemistry

Chemistry

ISBN:

9781305580350

Author:

William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote

Publisher:

Cengage Learning

Organic Chemistry

Chemistry

ISBN:

9781305080485

Author:

John E. McMurry

Publisher:

Cengage Learning

Organic Chemistry

Chemistry

ISBN:

9781305580350

Author:

William H. Brown, Brent L. Iverson, Eric Anslyn, Christopher S. Foote

Publisher:

Cengage Learning

SEE MORE TEXTBOOKS