After purification via extraction, any organic substance should be rigorously dried; otherwise, its further purification via recrystallization will often fail to achieve the desired result. In a typical purification of an organic unknown, a solution of crude product in an organic solvent (i.e. dichloromethane) is what will remain following extraction. Suggest a simple means to remove small quantities of water from this solution.
After purification via extraction, any organic substance should be rigorously dried; otherwise, its further purification via recrystallization will often fail to achieve the desired result. In a typical purification of an organic unknown, a solution of crude product in an organic solvent (i.e. dichloromethane) is what will remain following extraction. Suggest a simple means to remove small quantities of water from this solution.
Macroscale and Microscale Organic Experiments
7th Edition
ISBN:9781305577190
Author:Kenneth L. Williamson, Katherine M. Masters
Publisher:Kenneth L. Williamson, Katherine M. Masters
Chapter7: Extraction
Section: Chapter Questions
Problem 1Q
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![After purification via extraction, any organic substance should be rigorously dried; otherwise, its further purification via
recrystallization will often fail to achieve the desired result. In a typical purification of an organic unknown, a solution of crude
product in an organic solvent (i.e. dichloromethane) is what will remain following extraction. Suggest a simple means to remove
small quantities of water from this solution.](/v2/_next/image?url=https%3A%2F%2Fcontent.bartleby.com%2Fqna-images%2Fquestion%2F0077bb45-26df-400e-95c5-0803032f7a29%2F8cbf12e6-cdce-4751-9cef-27beca0482cc%2F8alpyc_processed.png&w=3840&q=75)
Transcribed Image Text:After purification via extraction, any organic substance should be rigorously dried; otherwise, its further purification via
recrystallization will often fail to achieve the desired result. In a typical purification of an organic unknown, a solution of crude
product in an organic solvent (i.e. dichloromethane) is what will remain following extraction. Suggest a simple means to remove
small quantities of water from this solution.
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