7. The level of ethyl acetate is determined in colchicines by headspace gas Answer: 0.055. in water was prepared. An aqueous standard containing 0.5912 mg/100 ml of ethyl acetate was also prepare. Headspace analysis of 2 ml volumes of the two solutions produced GC peaks for ethyl acetate with the following areas: Colchicines solution: Peak area 13457 Ethyl Acetate solution: Peak area 14689 Calculate the ethyl acetate content in the colchicines sample in pp,/

7. The level of ethyl acetate is determined in colchicines by headspace gas Answer: 0.055. in water was prepared. An aqueous standard containing 0.5912 mg/100 ml of ethyl acetate was also prepare. Headspace analysis of 2 ml volumes of the two solutions produced GC peaks for ethyl acetate with the following areas: Colchicines solution: Peak area 13457 Ethyl Acetate solution: Peak area 14689 Calculate the ethyl acetate content in the colchicines sample in pp,/

Appl Of Ms Excel In Analytical Chemistry

2nd Edition

ISBN:9781285686691

Author:Crouch

Publisher:Crouch

Chapter14: Chromatography

Section: Chapter Questions

Problem 9P

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Patients undergoing an upper gastrointestinal tract laboratory test are typically given an X-ray contrast agent that aids with the radiologic imaging of the anatomy. One such contrast agent is sodium diatrizoate, a nonvolatile water-soluble compound. A 0.378-m solution is prepared by dissolving 38.4 g sodium diatrizoate (NaDTZ) in.l.60 102 mL water at 3 1.2C (the density of water at 31.2C is 0.995 g/cm3). What is the molar mass of sodium diatrizoate? What is the vapor pressure of this solution if the vapor pressure of pure water at 31.2C is 34.1 torr?
The homogeneity of the chloride level in a water sample from a lake was tested by analyzing por- tions drawn from the top and from near the bottom of the lake, with the following results in ppm CI: Top 26.30 Bottom 26.22 26.43 26.32 26.28 26.20 26.19 26.11 26.49 26.42 (a) Apply the i test at the 95% confidence level to determine if the means are different. (b) Now use the paired / test and determine whether there is a significant difference between the top and bottom values at the 95% confidence level. (c) Why is a different conclusion drawn from using the paired i test than from just pooling the data and using the normal i test for differences in means?
What mass of MgCl₂ 6H₂O is required to make a 0.200 dm³ stock solution containing 25.0 ppm Mg(II)? What volumes of this stock solution are required to make 10.0 cm³ standard solutions containing 5.00, 1.00 and 0.10 ppm Mg(II)?
A sample of an infusion was diluted 10 ml to 250 ml and then 10 ml to 200 ml. It was thenanalysed and was found to contain sodium at 0.789 mg/100 ml. Calculate the concentrationof sodium in the original sample in %w/v. The sample was composed of a mixture of sodiumlactate and sodium carbonate in equimolar amounts. Calculate the amount of sodiumlactate and sodium carbonate in mg/10 ml of the sample (Na = 23, lactate = 89, carbonate =60)
A 500.0 μL aliquot of a ferric chloride solution is added to a 50.00 mL volumetric flask. To this flask is added 10 mL of 2M sodium acetate, 2 mL of 10 wt% NH4OCI, 3 mL of 5 wt% 1,10-phenanthroline, and enough DI water to fill the remaining volume of the flask for a total volume of 50.00 mL. Based on the UV-Visible light absorbance, the concentration of [Fe2+]=2.6 ppm. What is the concentration of Fe3+ ion in the original ferric chloride solution? O 3.85 X 103 ppm O 260.0 ppm O 260 ppm O 130 ppm
Calculate the osmolarity in mOsm/L of 500 mL of a solution containing 5% w/v dextrose, 0.78% w/v sodium chloride, and 27mEq of potassium acetate. dextrose: MW 180, # particles on dissociation 1 sodium chloride: MW 58.5, # particles on dissociation 2, valence 1 potassium acetate: MW 98, # particles on dissociation 2, valence 1
what are key reactions involved in seperation of liquid mixtures by simple and fractional distillation and gas chromatography? chemicals used: 10ml 1:1 mixture of ethyl and butyl acetate techniques: simple and fractional distillation, gas chromatography. target molecules: Ethyl acetate C4H8O2 Butyl acetate C6H12O2
A 100 ml bottle of metronidazole 100 mg/ml suspension is available in your pharmacy. Calculate the volume of this suspension needed to be diluted with cherry syrup to prepare 60 ml of a 4% metronidazole suspension. 1 ml of a 1:1000 epinephrine injection was mixed with 20 ml of 1% lidocaine injection. Calculate the new ratio strength of epinephrine in the admixture. (IGNORE ANY VOLUME CHANGES AFTER ADMIXTURE) Instead of preparing 4 grams of tetracaine hydrochloride 4% gel an 8% gel was compounded by mistake. How many grams of the 8% gel and gel base must be mixed to get 4 grams of a 4% gel? How many milliliters of 70% ethanol and 20% ethanol must be mixed to prepare 500 ml of 30% ethanol? A diphenhydramine elixir contains 12.5 mg drug in one teaspoon. The volume of oral vehicle that is to be added to 100 ml of this elixir to reduce its strength by one half its original strength is; 6. 90 capsules of Liothyronine (T3) 15 micrograms are to be prepared. The formula calls for a 1:10000…
1) How many milliliters of 70% ethanol and 20% ethanol must be mixed to prepare 500ml of 30% ethanol? 2) A gaseous blend of nitric oxide and nitrogen (NOmax) contains 0.09% v/v nitric oxide (NO) and 99.92% v/v nitrogen. Express the strength of nitric oxide in PPM (round to whole number) 3) The ratio strength of a 10mL vial of neostigmine methylsulfate injection USP is 1:1500.Calculate the amount of neostigmine methylsulfate in milligrams contained in the 10mL vial. (Round to the whole number).
Human saliva contains the enzyme α-amylase which hydrolyzes polysaccharide acetal linkages. A soda cracker (containing starch) was carefully ground; the crumbs were distributed evenly between two test tubes. The first test tube contained only water, while the second contained a 1% solution of α-amylase. Both mixtures were heated to 35°C for 10 minutes and filtered. The filtrates were tested with iodine solution and Benedict’s solution. Use the following results to answer the questions below. Mixture Iodine test Benedict’s Test cracker in water dark blue blue cracker in water and α-amylase red red-orange precipitate a. Was the starch from the cracker/water mixture hydrolyzed? Was the starch from the cracker in the 1% α-amylase solution hydrolyzed? b. Which cracker contained reducing sugars?
Researchers used gas chromatography to determine the % v/v methyl salicylate in rubbing alcohol [Van Atta, R. E.; Van Atta, R. L. J. Chem. Educ. 1980, 57, 230-231]. A set of standard additions was prepared by transferring 20.00 mL of rubbing alcohol to separate 25 - mL volumetric flasks and pipeting 0.00 mL, 0.20 mL, and 0.50 mL of methyl salicylate to the flasks. All three flasks were diluted to volume using isopropanol. Analysis of the three samples gave peak heights for methyl salicylate of 57.00 mm, 88.5 mm, and 132.5 mm, respectively. Determine the % v/v methyl salicylate in the rubbing alcohol.
The homogeneity of the chloride level in a water sample from a lake was tested by analyzing portions drawn from the top and from near the bottom of the lake, with the following results in ppm Cl: Apply the t test at the 95% confidence level to determine if the chloride level from the top of the lake is different from that at the bottom.