1) State if the following A student has already correctly identified his positive unknown tube. Ho pours some of his green, positive ion unknown into a clean centrifuge tube. He adds NaCl to this tubo and gets a precipitate. He centrifuges that precipitate and decants the clear liquid into a new clean testtube.. To that new tube, he adds Na,so and gets another precipitate. He centrifuges this tube, and decants the clear liquid into another clean, dry testtube. To this freshly decanted liquid, he adds NaOH and gets a third precipitate. This student concluded that he had Ag*, Ba*2 and Ni+2 in his positive ion unknown.

Fundamentals Of Analytical Chemistry
9th Edition
ISBN:9781285640686
Author:Skoog
Publisher:Skoog
Chapter20: Applications Of Oxidation/reduction Titrations
Section: Chapter Questions
Problem 20.6QAP
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1) State if the following technique and conclusions were correct. If not, what is wrong?
A student has already correctly identified his positive unknown tube. He pours some of his green,
positive ion unknown into a clean centrifuge tube. He adds NaCl to this tube and gets a precipitate.
He centrifuges that precipitate and decants the clear liquid into a new clean testtube. . To that new
tube, he adds Na,So, and gets another precipitate. He centrifuges this tube, and decants the
clear liquid into another clean, dry testtube. To this freshly decanted liquid, he adds NaOH and
gets a third precipitate.
This student concluded that he had Ag*,
Ba*2
and
+1
Ni+2
in his positive ion unknown.
Transcribed Image Text:1) State if the following technique and conclusions were correct. If not, what is wrong? A student has already correctly identified his positive unknown tube. He pours some of his green, positive ion unknown into a clean centrifuge tube. He adds NaCl to this tube and gets a precipitate. He centrifuges that precipitate and decants the clear liquid into a new clean testtube. . To that new tube, he adds Na,So, and gets another precipitate. He centrifuges this tube, and decants the clear liquid into another clean, dry testtube. To this freshly decanted liquid, he adds NaOH and gets a third precipitate. This student concluded that he had Ag*, Ba*2 and +1 Ni+2 in his positive ion unknown.
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