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Separation And Qualitative Analysis Of Cations Lab

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James Wood October 1, 2015 Experiment #05 Separation and Qualitative Analysis of Cations CHEM 1315-002 Purpose of the Experiment and Techniques: The purpose of this experiment is to qualitatively determine the substances that are present in several mixtures. This will be performed through analysis of ions present in the mixtures. In this experiment, six solutions will be tested through various methods, such as mixing with various other test solutions to indicate the presence of different cations. These tests will reveal what cations are present by whether or not it produces a precipitant or if the solution changes colors. Chemicals and Materials Required: This experiment employs the use of the following test solutions: 6 molar hydrochloric …show more content…

Equipment includes a hotplate, a centrifuge, and red and blue litmus paper. Caution should be expressed while handling or working with chemicals. Hydrochloric, nitric, sulfuric acids as well as ammonium hydroxide and sodium hydroxide, especially in such a high molarity, are extremely corrosive and will cause severe burns if brought into contact with the skin or eyes. Sodium bismuthate can cause damage to eyes and may be harmful if inhaled. Potassium thiocyanate can irritate skin and eyes. Experimental Procedures: Clean test tubes using distilled water and place in a test tube rack. Fill a 250mL beaker with water and place on a hotplate set to 200°C. Ensure the water stays between 70-80°C. Label clean test tubes 1-8. Add 3 drops of each cation solution to the test tube labeled “1”. Then, add 8 drops of hydrochloric acid to the test tube labeled “1” and stir. Check for the presence of a white precipitate. If a white precipitate exists, Ag+, Pb2+, and/or Hg22+ exist within the …show more content…

If more precipitate forms, continue to add hydrochloric acid until no more precipitant forms. Centrifuge once more and dispose of wash water. Add 1mL of distilled water to Test Tube 1. Heat the tube in the hot water bath for three minutes, stirring approximately every 30 seconds. Centrifuge while hot and decant the liquid from the tube quickly into Test Tube 2. Add 5 drops of sulfuric acid to Test Tube 2. If lead(II) ions are present, white precipitant will form. If lead is present, repeat the last four steps once again with test tube two until the white precipitate no longer

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